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Beilstein J. Org. Chem. 2013, 9, 2834–2840, doi:10.3762/bjoc.9.318
Graphical Abstract
Scheme 1: Synthesis of sulfonamide 3, N-alkylation of 3 in organic solution and of CD-complex (3β) in aqueous...
Figure 1: 2D NMR ROESY spectrum of the complex of 3 with β-CD in D2O, displaying the interaction of the tosyl...
Scheme 2: Cyclization of L-(+)-lysine monohydrochloride to give racemate 8.
Figure 2: Oscillatory rheological measurements of an equimolar mixture of 6 and 8 at 50 °C. Illustrated is th...
Beilstein J. Org. Chem. 2013, 9, 2803–2811, doi:10.3762/bjoc.9.315
Scheme 1: Synthesis of the monomers 5 and 7, as well as the chemical structure of the diepoxide 8, comprising...
Figure 1: Heating curves of the LCST measurements of 9, the complex of 9 with RAMEB-CD 9β, and of 9 with RAME...
Figure 2: LCST measurements of 10 with illustrated heating and cooling curve, as well as the heating curve af...
Figure 3: 2D NMR ROESY (300 MHz, D2O) spectrum of the complex of 5 with RAMEB-CD (a), displaying the correlat...
Figure 4: Oscillatory rheological measurements of the curing of 9 and 10, respectively at 25 °C. Illustrated ...
Figure 5: Illustration of the viscosity of a mixture of 5 and 8 (a), respectively 7 and 8 (c) before curing a...
Figure 6: Comparison of the FTIR spectra of the monomer mixture of 5 and 8 and of the cured product 9 after 2...